HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 55288024, compound → HCID 67789778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 55288024 | HCID 55288024 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67789778 | HCID 67789778 | 98.6% |
Reaction Steps
A solution of trans-3-(1-hydroxyethyl)-4-ethynyl-2-azetidinone (0.10 g) in ethanol (5 ml) is subjected to catalytic reduction with hydrogen gas in the presence of Lindlar catalyst (0.01 g). The reduction is continued until 14 ml of hydrogen gas has been absorbed. The catalyst is then filtered off and the filtrate is concentrated under reduced pressure to give 0.1 g of trans-3-(1-hydroxyethyl)-4-vinyl-2-azetidinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845210 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-9a0203573c4745878a1572f5f764ca60 |
| Source note | uspto-grants-1989_07 |