Toluene → HCID 14498225, compound

Participants

Reaction Steps

Into 10 ml of toluene containing 2 g of trimethylamine is dissolved 1.0 g of 2-mesyloxyethyl 2-methoxy-3-octadecyloxypropyl sulfone and the solution is stirred at room temperature for 6 hours. Then 30 ml of hexane is added to the mixture and precipitates are removed by filtration. The filtrate is concentrated to give 0.6 g of the captioned compound as colorless crystals (m.p.47°-49° C.).

Provenance & Evidence