HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → HCID 14498256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | 3-Mesyloxypropyl 2-methoxy-3-(12-cyclohexyldodecyloxy)propyl sulfone | HCID 20034848 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14498256 | HCID 14498256 | — |
Reaction Steps
In 50 ml of toluene containing 10 g of trimethylamine is dissolved 5.4 g of 3-mesyloxypropyl 2-methoxy-3-(12-cyclohexyldodecyloxy)propyl sulfone, and the mixture is stirred at room temperature for 5 days. The reaction mixture is then concentrated to dryness and the residue is purified by silica gel column chromatography to obtain 3.17 g of the captioned compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845219 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-bf3981c375a8487e95b82749d95f8906 |
| Source note | uspto-grants-1989_07 |