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HRID23129

反应详情

EQUATION

反应方程式

HRID 23129 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccccc1
HCID6115

Aniline

C6H7N

结构：O=C(Cl)C=Cc1ccccc1
HCID66023

3-Phenylprop-2-enoyl chloride

C9H7ClO

PRODUCTS

生成物

1
结构：O=C1CC(c2ccccc2)c2ccccc2N1
HCID272509

4-phenyl-3,4-dihydroquinolin-2(1h)-one

C15H13NO

PROCEDURE

实验过程

4-Phenyl-3,4-dihydrocarbostyril (CAS# 4888-33-9) was prepared in two steps using the procedure described by Conley, R. T.; Knopka. W. N. J. Org. Chem. 1964, 29, 496-497. The starting materials for this preparation were cinnamoyl chloride (Aldrich) and aniline (Aldrich). The title compound was purified by flash chromatography eluting with CH2Cl2/EtOAc (4:1).

WORKUP

后处理

  1. customThe title compound was purified by flash chromatography
  2. washeluting with CH2Cl2/EtOAc (4:1)