Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Methyl 2-pentenoate | HCID 5364718 | — |
| Product | Methyl 3-piperidinovalerate | HCID 14178339 | 64.5% |
Reaction Steps
A mixture of 500 g of methyl 2-trans-pentenoate and 372 g of piperidine was heated at 100° C. for 24 hours. 562 g (64% of theory) of methyl 3-piperidinovalerate of boiling point 75°-77° C./2 mbar were obtained by fractional distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04845269 |
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| Source dataset | uspto-grants-1989_07 |
|---|
| ORD ID | ord-1785ac3550ef49e892064cbec520e176 |
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| Source note | uspto-grants-1989_07 |
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