HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoprene → HCID 15664015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoprene | HCID 6557 | — |
| Reactant | 2,6-Diaminotoluene | HCID 13205 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | HCID 15664015 | HCID 15664015 | — |
Reaction Steps
A 200g (1.64 mol) portion of 2,6-toluenediamine, 167g (2.45 mol) of isoprene, 200g (2.78 mol) of pentane, and 20g of powdered H-Y zeolite were reacted at 150° C. in a similar fashion as indicated in Example 3. Isolation of a catalyst free sample was obtained by hot filtration. Selective removal of all residual hydrocarbon by vacuum distillation afforded the following product mixture:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845291 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-2163a6ca6cd7480aa715ce4158821471 |
| Source note | uspto-grants-1989_07 |