Isoprene → HCID 86743223, compound

Participants

Reaction Steps

1,2-Phenylenediamine (200g, 1.85 mol), 189g (2.77 mol) of isoprene, 225g (3.14 mol) of pentane and 20g of 13 wt% alumina/87 wt% silica catalyst were reacted in a fashion similar to example 1. The reaction was conducted at 200° C. for 24 hr. with an initial pressure of 426 psig. Product analysis by gas chromatography on isoprene and pentane free sample afforded by the following assay.

Provenance & Evidence