HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → (2,4-Dichloro-5-nitrophenyl)methyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1,5-Dichloro-2-methyl-4-nitrobenzene | HCID 251679 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | (2,4-Dichloro-5-nitrophenyl)methyl bromide | HCID 14501785 | — |
Reaction Steps
This compound was prepared in a manner similar to Example 1 Step F using 2,4-dichloro-5-nitrotoluene (62.0 g, 0.3 mole), N-bromosuccinimide (160.2 g, 0.9 mole), benzoyl peroxide (2.0 g) and carbon tetrachloride (500 ml) to yield (2,4-dichloro-5-nitrophenyl)methyl bromide. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04846875 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-b2fd7d6809ae443fa2e3d2bbc9fa27eb |
| Source note | uspto-grants-1989_07 |