反应详情

By the method of Example 2, Step H, 0.50 g (0.0020 mole) of 4-chloro-2-fluoro-5-(diisopropylaminomethyl)aniline and 0.85 g (0.0056 mole) of tetrahydrophthalic anhydride in 20 ml of acetic acid were reacted yielding 0.052 g of N-[4-chloro-2-fluoro-5-(diisopropylaminomethyl)phenyl]-3,4,5,6-tetrahydrophthalimide. The nmr and ir spectra were consistent with the proposed structure.