HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-bromobutanimide → 1-(Bromomethyl)-2-chloro-4-fluorobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | 2-Chloro-4-fluorotoluene | HCID 96747 | — |
| Katalysator | Benzoyl Peroxide | HCID 7187 | — |
| Lösungsmittel | Carbon Tetrachloride | HCID 5943 | — |
| Produkt | 1-(Bromomethyl)-2-chloro-4-fluorobenzene | HCID 2725062 | 75,5% |
Reaktionsschritte
By the method of Example 7, Step C, 141.4 g (0.978 mole) of 2-chloro-4-fluorotoluene, 175.8 g (0.978 mole) of N-bromosuccinimide, and 5.0 g of benzoyl peroxide in 15 liters of carbon tetrachloride were reacted, yielding 165 g of 2-chloro-4-fluorobenzyl bromide as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04846882 |
| Quelldatensatz | uspto-grants-1989_07 |
| ORD ID | ord-92bbe4b3fa884de7adea63d2004552e8 |
| Quellennotiz | uspto-grants-1989_07 |