HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14254887, compound → HCID 20032923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14254887 | HCID 14254887 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20032923 | HCID 20032923 | — |
Reaction Steps
2 g. (8.3 mmole) of the compound prepared in Example 2 were boiled in 250 ml. dioxan with 50 g. pyrolusite for 5 hours, filtered off with suction and the filtrate concentrated until it crystallised. After recrystallisation from ethanol, there was obtained 1 g. of the title compound; m.p. 300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04847251 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-5a3642c97d8a4b84a1e5ead68b7d9900 |
| Source note | uspto-grants-1989_07 |