HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Allyl-6-t-butylphenol → 2-n-Propyl-6-t-butylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Allyl-6-t-butylphenol | HCID 520641 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-n-Propyl-6-t-butylphenol | HCID 14672043 | 98% |
Reaction Steps
A solution of 2-allyl-6-t-butylphenol (1.9 g) (see Example 3) in 100 ml MeOH is hydrogenated in a Parr system for 75 min at 25° C. (50 psi of H2). The mixture is then filtered and concentrated in vacuo to give 2-n-propyl-6-t-butylphenol (1.88 gram; 98% yield), which is used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04847303 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-acc39d64781e44448ee2b68c7a87554b |
| Source note | uspto-grants-1989_07 |