Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Isocyanate → Aldicarb [ISO]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Isocyanate | HCID 12228 | — |
| 반응물 | 2-Methylthio-2-methylpropionaldoxime | HCID 15436 | — |
| 생성물 | Aldicarb [ISO] | HCID 2086 | — |
반응 단계
The process of this invention can be carried out by contacting 2-methyl-2-(methylthio) propionaldehyde oxime with methyl isocyanate in the presence of an aqueous medium for a period sufficient to form 2-methyl-2-(methylthio) propionaldehyde O-(methylcarbamoyl) oxime which is reacted with a mixture of hydrogen peroxide and a carboxylic acid in the presence of an agueous medium and a catalyst, i.e., mineral or organic sulfonic acid, to give 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl) oxime as a solid in an agueous slurry which is then filtered to give a water-wet cake.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04847413 |
| 출처 데이터셋 | uspto-grants-1989_07 |
| ORD ID | ord-c2719d408f8b474cad74e3a43b2cd2e5 |
| 출처 메모 | uspto-grants-1989_07 |