HCID 20033670, compound → HCID 20033697, compound
Reaction equation
C(CC[C:6]1[CH:11]=[CH:10][C:9]([S:12]([C:15]2[S:19][C:18]([S:20]([NH2:23])(=[O:22])=[O:21])=[CH:17][CH:16]=2)(=[O:14])=[O:13])=[CH:8][CH:7]=1)(O)=O.[C:24]([CH2:27]CCC1C=CC(S(C2SC(S(N)(=O)=O)=CC=2)(=O)=O)=CC=1)([OH:26])=[O:25]>>[C:24]([CH2:27][C:6]1[CH:11]=[CH:10][C:9]([S:12]([C:15]2[S:19][C:18]([S:20]([NH2:23])(=[O:22])=[O:21])=[CH:17][CH:16]=2)(=[O:13])=[O:14])=[CH:8][CH:7]=1)([OH:26])=[O:25]Participants
3
Procedure
In a similar manner 5-[4-(2-carboxyethyl)phenylsulfonyl]thiophene-2-sulfonamide (m.p. 195°-197° C.) and 5-[4-(3-carboxypropyl)phenylsulfonyl]thiophene-2-sulfonamide (m.p. 124°-126° C.) were synthesized.
Sources & evidence
- ORD record
- ord-cff120ade1684118a45573a05596361d
- Source dataset
- uspto-grants-1989_07
- Patent number
- US04847289
Reaction notes
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