HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Cyclopentanecarboxaldehyde, 2,2,5,5-tetramethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2,2,5,5-Tetramethylcyclopentylidenemethyl methyl ether | HCID 13922942 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Cyclopentanecarboxaldehyde, 2,2,5,5-tetramethyl- | HCID 9793878 | 94% |
Reaction Steps
10 g of 2,2,5,5-tetramethylcyclopentylidenemethyl methyl ether was dissolved in 100 ml of tetrahydrofuran, and 50 ml of 6N-hydrochloric acid was added thereto. The mixture was vigorously stirred at room temperature for 3 hours, and then treated in the same manner as in Example 11 to obtain 8.60 g of 1-formyl-2,2,5,5-tetramethylcyclopentane. Yield 94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04847390 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-d60cc9c2e1af47f7ac38d442034f479d |
| Source note | uspto-grants-1989_07 |