Ethylenediamine → HCID 20031853, compound

Participants

Reaction Steps

To a vigorously shaken solution of 1.39 g of ethylene diamine in 20 ml of water and 20 ml of tetrahydrofuran was added over 45 minutes a solution of 5 g of 4-nitrobenzyl chloroformate in 20 ml of dioxane. The mixture was allowed to warm to room temperature, and 150 ml of ethyl acetate and 200 ml of water were added. The mixture was filtered, and the filtrate dried to afford 2.67 g of the title compound.

Provenance & Evidence