HRID231985

反应详情

EQUATION

反应方程式

HRID 231985 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

On the other hand, 38 g of stannous chloride, 26 g of lead acetate and 200 g of water were charged into a 500 ml beaker equipped with a stirrer and the metal salts were dissolved into the water with stirring. This aqueous solution of the metal salts was added to the aforesaid aqueous solution of potassium naphthenate and a double decomposition reaction was then carried out for 1 hour at 30° C. The reaction mixture was dehydrated, dried and then extracted with toluene. The residue was heated under a reduced pressure of 10 mm Hg to distill off the toluene whereby stannous and lead naphthenates were obtained which had a tin content of 13.2% by weight and a lead content of 9.2% by weight.

WORKUP

后处理

  1. custombeaker equipped with a stirrer
  2. customa double decomposition reaction
  3. customdried
  4. extractionextracted with toluene
  5. temperatureThe residue was heated under a reduced pressure of 10 mm Hg
  6. distillationto distill off the toluene whereby stannous