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HRID232187

反应详情

EQUATION

反应方程式

HRID 232187 的结构方程式

REACTANTS

反应物

3
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：OCC(O)CBr
HCID20827

3-Bromopropane-1,2-diol

C3H7BrO2

结构：O=S(=O)([O-])[O-].[Mg+2]
HCID24083

Magnesium sulfate anhydrous

MgO4S

PRODUCTS

生成物

1
结构：CC1(C)OCC(CBr)O1
HCID169759

4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane

C6H11BrO2

PROCEDURE

实验过程

An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.

WORKUP

后处理

  1. customThe cooled reaction mixture
  2. filtrationis filtered
  3. customthe solvent is removed