Veratroyl chloride → HCID 20031372, compound

HRID 232285Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6](Cl)=[O:7].[N:14]1([CH:20]([CH3:33])[CH2:21][CH2:22][NH:23][C:24]2[CH:29]=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=2)[CH2:19][CH2:18][O:17][CH2:16][CH2:15]1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([N:23]([CH2:22][CH2:21][CH:20]([N:14]1[CH2:15][CH2:16][O:17][CH2:18][CH2:19]1)[CH3:33])[C:24]1[CH:25]=[CH:26][C:27]([N+:30]([O-:32])=[O:31])=[CH:28][CH:29]=1)=[O:7]

Participants

Reactant 2

HCID 77070Veratroyl chloride

HCID 20031354HCID 20031354, compound

Product 1

HCID 20031372HCID 20031372, compound

Procedure

In a manner similar to Preparation 16, react 3,4-dimethoxybenzoyl chloride with N-[3-(morpholin-4-yl)butyl]-4-nitrobenzenamine to obtain the title compound.

Workup

customIn a manner similar to Preparation 16

Sources & evidence

ORD record: ord-09d5493fa56f4a4dbaeecb59f81e57ed
Source dataset: uspto-grants-1989_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04851526

Reaction notes

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