p-Fluoronitrobenzene → HCID 54010549, compound

HRID 232289Notes

Reaction equation

HRID 232289 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[NH2:11][CH2:12][CH:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH:14]1[N:19]([CH2:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)[CH2:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([NH:11][CH2:12][CH:13]2[CH2:18][CH2:17][CH2:16][CH2:15][CH:14]2[N:19]([CH2:27][C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)[CH2:20][C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)=[CH:3][CH:4]=1)([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 20031402HCID 20031402, compound

Product 1

HCID 54010549HCID 54010549, compound

Procedure

In a manner similar to Preparation 2, react 1-fluoro-4-nitrobenzene with N-[2-(aminomethyl)cyclohexyl]-N-(phenylmethyl)benzenemethanamine to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-11d1f51a4bfb45e4bc0f9bc9547f68b6
Source dataset
uspto-grants-1989_07
Patent number
US04851526

Reaction notes

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