HCID 14555653, compound → HCID 14555622, compound

HRID 232320Notes

Reaction equation

HRID 232320 reaction equation
[CH2:1]([N:4]([CH2:24][CH2:25][CH3:26])[CH2:5][CH2:6][C:7]([N:9]([C:13]1[CH:18]=[CH:17][C:16]([N:19]2[CH:23]=[CH:22][N:21]=[CH:20]2)=[CH:15][CH:14]=1)[CH2:10][CH:11]=[CH2:12])=O)[CH2:2][CH3:3].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH2:24]([N:4]([CH2:1][CH2:2][CH3:3])[CH2:5][CH2:6][CH2:7][N:9]([C:13]1[CH:14]=[CH:15][C:16]([N:19]2[CH:23]=[CH:22][N:21]=[CH:20]2)=[CH:17][CH:18]=1)[CH2:10][CH:11]=[CH2:12])[CH2:25][CH3:26]

Participants

3

Reactant 2

HCID 14555653HCID 14555653, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 14555622HCID 14555622, compound

Procedure

In a manner similar to Preparation 4, react 3-(dipropylamino)-N-[4-(1H-imidazol-yl)phenyl]-N-(2-propenyl)propanamide with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 4

Sources & evidence

ORD record
ord-b06d0c1453964c53ba77c81e616c8edd
Source dataset
uspto-grants-1989_07
Patent number
US04851526

Reaction notes

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