Hydrazine → HCID 14555632, compound

HRID 232325Notes

Reaction equation

HRID 232325 reaction equation
[CH3:1][N:2]([CH3:22])[CH:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH:4]1[C:9]([C:11]1[CH:16]=[CH:15][C:14]([N:17]2[CH:21]=[CH:20][N:19]=[CH:18]2)=[CH:13][CH:12]=1)=O.[OH-].[K+].NN>C(O)COCCO>[CH3:22][N:2]([CH3:1])[CH:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH:4]1[CH2:9][C:11]1[CH:12]=[CH:13][C:14]([N:17]2[CH:21]=[CH:20][N:19]=[CH:18]2)=[CH:15][CH:16]=1

Participants

5

Reactant 3

HCID 9321HydrazineHCID 14797Potassium HydroxideHCID 14555630HCID 14555630, compound

Product 1

HCID 14555632HCID 14555632, compound

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In a manner similar to Example 28, react [2-(dimethylamino)cyclohexyl][4-(1H-imidazol-1-yl)phenyl]methanone with potassium hydroxide and hydrazine in diethylene glycol to obtain the title compound.

Sources & evidence

ORD record
ord-774dd320aeb74beba21b942a8a77213f
Source dataset
uspto-grants-1989_07
Patent number
US04851526

Reaction notes

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