Hydrazine → HCID 14555635, compound

HRID 232327Notes

Reaction equation

HRID 232327 reaction equation
[CH2:1]([N:3]([CH2:6][CH:7]1[CH2:9][CH:8]1[C:10]([C:12]1[CH:17]=[CH:16][C:15]([N:18]2[CH:22]=[CH:21][N:20]=[CH:19]2)=[CH:14][CH:13]=1)=O)[CH2:4][CH3:5])[CH3:2].[OH-].[K+].NN>C(O)COCCO>[CH2:4]([N:3]([CH2:1][CH3:2])[CH2:6][CH:7]1[CH2:9][CH:8]1[CH2:10][C:12]1[CH:17]=[CH:16][C:15]([N:18]2[CH:22]=[CH:21][N:20]=[CH:19]2)=[CH:14][CH:13]=1)[CH3:5]

Participants

5

Reactant 3

HCID 9321HydrazineHCID 14797Potassium HydroxideHCID 14555633HCID 14555633, compound

Product 1

HCID 14555635HCID 14555635, compound

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

In a manner similar to Example 28, react [2-[(diethylamino)methyl]cyclopropyl][4-(1H-imidazol-1-yl)phenyl]-methanone with potassium hydroxide and hydrazine in diethylene glycol to obtain the title compound.

Sources & evidence

ORD record
ord-29ad07c6fcba4d0783d4160c63574872
Source dataset
uspto-grants-1989_07
Patent number
US04851526

Reaction notes

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