HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Sulfuric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Sulfuric Acid | HCID 1118 | — |
| Product | Dicyclohexylamine | HCID 7582 | — |
Reaction Steps
In a Meyer's flask having an inner volume of 300 ml, 100 g of orthoxylene and 60 g of sulfuric acid were dispersed. Then the Meyer's flask was kept cooled in a water bath, 122 g of cyclohexylamine was added dropwise thereto to obtain a xylene slurry of white crystals of dicyclohexylamine salt of sulfuric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851547 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-6eafb3769aed4060bef25d376a149b84 |
| Source note | uspto-grants-1989_07 |