HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53878961, compound → HCID 54385336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53878961 | HCID 53878961 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54385336 | HCID 54385336 | — |
Reaction Steps
A solution of 0.28 of 5'-(2-azidoethyl)-2',5'-dideoxy-5-ethyluridine in 50 ml of ethanol was hydrogenated over 50 mg of 10% palladium-on-carbon catalyst for 2 hours. The catalyst was removed by filtration and the filtrate was evaporated to dryness to give 0.23 g of 5'-(2-aminoethyl)-2',5'-dideoxy-5-ethyluridine in the form of a colorless oil which crystallized upon standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851519 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-bd4a13507dc549db8541adc39fc822ee |
| Source note | uspto-grants-1989_07 |