Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | 1-Bromooctadecane | HCID 8218 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Distearyl Ether | HCID 80526 | — |
Reaction Steps
Distearyl ether was synthesized by reacting stearyl bromide (Sigma) with PEG-900 in the presence of potassium hydroxide. Stearyl bromide (4.168 g in 10 ml toluene) was slowly added with stirring to 4.64 g of PEG-900 in 10 ml of toluene at 45° C. The mixture was then stirred at 60° C. for 30 min. and refluxed for 6 hrs. The final product was treated with charcoal, filtered and isolated from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05591715 |
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| Source dataset | uspto-grants-1997_01 |
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| ORD ID | ord-3cf91bd8c78b45ccbe106bf28b4ddeb1 |
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| Source note | uspto-grants-1997_01 |
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