2-Ethoxybenzoyl chloride → HCID 22462351, compound

HRID 232570Notes

Reaction equation

HRID 232570 reaction equation
[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=1[C:6](Cl)=[O:7])[CH3:2].[NH2:13][C:14]1[C:15]([C:20]([NH2:22])=[O:21])=[N:16][CH:17]=[CH:18][CH:19]=1>>[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=1[C:6]([NH:13][C:14]1[C:15]([C:20]([NH2:22])=[O:21])=[N:16][CH:17]=[CH:18][CH:19]=1)=[O:7])[CH3:2]

Participants

3

Reactant 2

HCID 30163972-Ethoxybenzoyl chlorideHCID 132387253-Amino-pyridine-2-carboxylic acid amide

Product 1

HCID 22462351HCID 22462351, compound

Procedure

The title compound was prepared from 2-ethoxybenzoyl chloride and 3-aminopyridine-2-carboxamide (J. Chem. Soc., 1956, 1045) following the procedure of Preparation 7 and was obtained as an off-white solid (100 %), m.p. 172°-177° C. Found: C,62.91; H,5.30; N,14.51. C15H15N3O3 requires C,63.15; H,5.30; N,14.73%.

Workup

  1. customthe procedure of Preparation 7

Sources & evidence

ORD record
ord-6249c5d979384a68aa0511caccd50deb
Source dataset
uspto-grants-1997_01
Patent number
US05591742

Reaction notes

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