HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → 2,3,4,5-Tetrafluoro-6-methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | 2,3,4,5-Tetrafluoro-6-methylbenzoic acid | HCID 12943997 | — |
| Product | 2,3,4,5-Tetrafluoro-6-methylbenzoyl chloride | HCID 14651256 | — |
Reaction Steps
To 6-methyl-2,3,4,5-tetrafluorobenzoic acid (5.60 g) is added thiony chloride (9.8 ml) and the mixture is refluxed for 1 hour. After concentrating, 6-methyl-2,3,4,5-tetrafluorobenzoyl chloride (5.20 g) is obtained as a colorless oil, b.p. 82° C./23 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591744 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-e82a0650db9347bb99fe2fc522b08403 |
| Source note | uspto-grants-1997_01 |