HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 86750121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86750122 | HCID 86750122 | — |
| Product | HCID 86750121 | HCID 86750121 | 91.1% |
Reaction Steps
16β-(1,4-Dioxa-8-azaspiro[4.5]dec-8-yl)-2α,3α-epoxy-5α-androstan-17-one is reduced by using sodium borohydride as described in Example 2 to give the title compound in a yield of 91.1%, m.p.: 186°-188° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591735 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-57e9941a219d42bca7e130e91d600c95 |
| Source note | uspto-grants-1997_01 |