Acetyl chloride → HCID 23360853, compound

HRID 232781Notes

Reaction equation

HRID 232781 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH2:13][CH2:14][NH:15][C:16]([CH:18]2[CH2:20][CH2:19]2)=[O:17])=[CH:5][CH:4]=1.[C:21](Cl)(=[O:23])[CH3:22]>>[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[C:8]([C:21](=[O:23])[CH3:22])[CH:9]=[C:10]2[CH2:13][CH2:14][NH:15][C:16]([CH:18]2[CH2:19][CH2:20]2)=[O:17])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 164405N-Cyclopropylcarbonyl-2-(7-methoxy-1-naphthyl)ethylamine

Product 1

HCID 23360853HCID 23360853, compoundYield 31%

Procedure

By working as in Example 1, using N-[2-(7-methoxynaphth-1-yl)ethyl]cyclopropylcarboxamide and acetyl chloride as starting materials, the compound of Example 50 is obtained.

Sources & evidence

ORD record
ord-0ac0c20d5795443390de5b4ec3366773
Source dataset
uspto-grants-1997_01
Patent number
US05591775

Reaction notes

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