HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(5-Aminopentyl)phenol-hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11507342 | HCID 11507342 | — |
| Product | 4-(5-Aminopentyl)phenol-hydrochloride | HCID 19433645 | — |
Reaction Steps
20.8 g of 4-(5-aminopentyl)anisole are heated with 350 ml of semiconcentrated hydrochloric acid in a glass bomb for 10 hours to 180° C. The solution is concentrated by evaporation in vacuo, the residue is dissolved in ethanol and treated with activated charcoal. The residue remaining after evaporation is used further as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591769 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-78fd134132fb4aaab3a5e00ac3de4fca |
| Source note | uspto-grants-1997_01 |