3-Mercaptopropionic Acid → HCID 23359221, compound

HRID 232829Notes

Reaction equation

HRID 232829 reaction equation
[F:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH2:12][O:13][C:14]1[CH:29]=[CH:28][C:17]3[O:18][CH2:19][C:20]4[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=4[CH:22](O)[C:16]=3[CH:15]=1)[CH:6]=[CH:5]2.[SH:30][CH2:31][CH2:32][C:33]([OH:35])=[O:34]>>[C:33]([CH2:32][CH2:31][S:30][CH:22]1[C:21]2[CH:24]=[CH:25][CH:26]=[CH:27][C:20]=2[CH2:19][O:18][C:17]2[CH:28]=[CH:29][C:14]([O:13][CH2:12][C:7]3[CH:6]=[CH:5][C:4]4[C:9](=[CH:10][CH:11]=[C:2]([F:1])[CH:3]=4)[N:8]=3)=[CH:15][C:16]1=2)([OH:35])=[O:34]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 23359150HCID 23359150, compound

Product 1

HCID 23359221HCID 23359221, compound

Procedure

2-(6-Fluoroquinolin-2-yl)methoxy-11-hydroxy-6,11-dihydrodibenz[b,e]oxepine and 3-mercaptopropionic acid were used and reacted in the same manner as in Example 1 to obtain the title compound.

Workup

  1. customreacted in the same manner as in Example 1

Sources & evidence

ORD record
ord-9d31d7350dbf4e47bcb3cec27ce09305
Source dataset
uspto-grants-1997_01
Patent number
US05591752

Reaction notes

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