3-Mercaptopropionic Acid → HCID 23359218, compound

HRID 232832Notes

Reaction equation

HRID 232832 reaction equation
[F:1][CH:2]([F:32])[O:3][C:4]1[CH:13]=[C:12]2[C:7]([CH:8]=[CH:9][C:10]([CH2:14][O:15][C:16]3[CH:31]=[CH:30][C:19]4[O:20][CH2:21][C:22]5[CH:29]=[CH:28][CH:27]=[CH:26][C:23]=5[CH:24](O)[C:18]=4[CH:17]=3)=[N:11]2)=[CH:6][CH:5]=1.[SH:33][CH2:34][CH2:35][C:36]([OH:38])=[O:37]>>[C:36]([CH2:35][CH2:34][S:33][CH:24]1[C:23]2[CH:26]=[CH:27][CH:28]=[CH:29][C:22]=2[CH2:21][O:20][C:19]2[CH:30]=[CH:31][C:16]([O:15][CH2:14][C:10]3[CH:9]=[CH:8][C:7]4[C:12](=[CH:13][C:4]([O:3][CH:2]([F:32])[F:1])=[CH:5][CH:6]=4)[N:11]=3)=[CH:17][C:18]1=2)([OH:38])=[O:37]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 23359187HCID 23359187, compound

Product 1

HCID 23359218HCID 23359218, compound

Procedure

2-(7-Difluoromethoxyquinolin-2-yl)methoxy-11-hydroxy-6,11-dihydrodibenz[b,e]oxepine and 3-mercaptopropionic acid were used and reacted in the same manner as in Example 1 to obtain the title compound.

Workup

  1. customreacted in the same manner as in Example 1

Sources & evidence

ORD record
ord-00eb6f2c2c5441bb986c5d31c5bd284a
Source dataset
uspto-grants-1997_01
Patent number
US05591752

Reaction notes

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