3-Mercaptopropionic Acid → HCID 23359228, compound

HRID 232833Notes

Reaction equation

HRID 232833 reaction equation
[F:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:11]=1[N:10]=[C:9]([CH2:12][O:13][C:14]1[CH:29]=[CH:28][C:17]3[O:18][CH2:19][C:20]4[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=4[CH:22](O)[C:16]=3[CH:15]=1)[CH:8]=[CH:7]2.[SH:30][CH2:31][CH2:32][C:33]([OH:35])=[O:34]>>[C:33]([CH2:32][CH2:31][S:30][CH:22]1[C:21]2[CH:24]=[CH:25][CH:26]=[CH:27][C:20]=2[CH2:19][O:18][C:17]2[CH:28]=[CH:29][C:14]([O:13][CH2:12][C:9]3[CH:8]=[CH:7][C:6]4[C:11](=[C:2]([F:1])[CH:3]=[CH:4][CH:5]=4)[N:10]=3)=[CH:15][C:16]1=2)([OH:35])=[O:34]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 23359185HCID 23359185, compound

Product 1

HCID 23359228HCID 23359228, compound

Procedure

2-(8-Fluoroquinolin-2-yl)methoxy-11-hydroxy-6,11-dihydrodibenz[b,e]oxepine and 3-mercaptopropionic acid were used and reacted in the same manner as in Example 1 to obtain the title compound.

Workup

  1. customreacted in the same manner as in Example 1

Sources & evidence

ORD record
ord-eb4480879c494fd3b98387f7622665bd
Source dataset
uspto-grants-1997_01
Patent number
US05591752

Reaction notes

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