3-Mercaptopropionic Acid → HCID 23359202, compound

HRID 232834Notes

Reaction equation

HRID 232834 reaction equation
[CH2:1]([C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH2:13][O:14][C:15]1[CH:30]=[CH:29][C:18]3[O:19][CH2:20][C:21]4[CH:28]=[CH:27][CH:26]=[CH:25][C:22]=4[CH:23](O)[C:17]=3[CH:16]=1)[CH:7]=[CH:6]2)[CH3:2].[SH:31][CH2:32][CH2:33][C:34]([OH:36])=[O:35]>>[C:34]([CH2:33][CH2:32][S:31][CH:23]1[C:22]2[CH:25]=[CH:26][CH:27]=[CH:28][C:21]=2[CH2:20][O:19][C:18]2[CH:29]=[CH:30][C:15]([O:14][CH2:13][C:8]3[CH:7]=[CH:6][C:5]4[C:10](=[CH:11][CH:12]=[C:3]([CH2:1][CH3:2])[CH:4]=4)[N:9]=3)=[CH:16][C:17]1=2)([OH:36])=[O:35]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 23359233HCID 23359233, compound

Product 1

HCID 23359202HCID 23359202, compound

Procedure

2-(6-Ethylquinolin-2-yl)methoxy-11-hydroxy-6,11-dihydrodibenz[b,e]oxepine and 3-mercaptopropionic acid were used and reacted in the same manner as in Example 1 to obtain the title compound.

Workup

  1. customreacted in the same manner as in Example 1

Sources & evidence

ORD record
ord-00466ce2040c43c0981068e2670dc028
Source dataset
uspto-grants-1997_01
Patent number
US05591752

Reaction notes

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