Benzenesulfonyl chloride → HCID 23359197, compound

HRID 232854Notes

Reaction equation

[NH2:1][CH2:2][CH2:3][S:4][CH:5]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[CH2:9][O:8][C:7]2[CH:16]=[CH:17][C:18]([O:20][CH2:21][C:22]3[CH:31]=[CH:30][C:29]4[C:24](=[CH:25][C:26]([Cl:32])=[CH:27][CH:28]=4)[N:23]=3)=[CH:19][C:6]1=2.[C:33]1([S:39](Cl)(=[O:41])=[O:40])[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>>[C:33]1([S:39]([NH:1][CH2:2][CH2:3][S:4][CH:5]2[C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=3[CH2:9][O:8][C:7]3[CH:16]=[CH:17][C:18]([O:20][CH2:21][C:22]4[CH:31]=[CH:30][C:29]5[C:24](=[CH:25][C:26]([Cl:32])=[CH:27][CH:28]=5)[N:23]=4)=[CH:19][C:6]2=3)(=[O:41])=[O:40])[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1

Participants

Reactant 2

HCID 7369Benzenesulfonyl chloride

HCID 23359139HCID 23359139, compound

Product 1

HCID 23359197HCID 23359197, compound

Procedure

11-(2-Aminoethylthio)-2-(7-chloroquinolin-2-yl)methoxy-6,11-dihydrodibenz[b,e]oxepine and phenylsulfonyl chloride were used and reacted in the same manner as in Example 34 to obtain the title compound.

Workup

customreacted in the same manner as in Example 34

Sources & evidence

ORD record: ord-d21f7a28302b469990b654c4d1aa38af
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05591752

Reaction notes

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