3-Mercaptopropionic Acid → HCID 23359128, compound

HRID 232862Notes

Reaction equation

HRID 232862 reaction equation
[Cl:1][C:2]1[C:11]([F:12])=[CH:10][CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][C:6]([CH2:13][O:14][C:15]1[CH:30]=[CH:29][C:18]3[O:19][CH2:20][C:21]4[CH:28]=[CH:27][CH:26]=[CH:25][C:22]=4[CH:23](O)[C:17]=3[CH:16]=1)=[N:7]2.[SH:31][CH2:32][CH2:33][C:34]([OH:36])=[O:35]>>[C:34]([CH2:33][CH2:32][S:31][CH:23]1[C:22]2[CH:25]=[CH:26][CH:27]=[CH:28][C:21]=2[CH2:20][O:19][C:18]2[CH:29]=[CH:30][C:15]([O:14][CH2:13][C:6]3[CH:5]=[CH:4][C:3]4[C:8](=[CH:9][CH:10]=[C:11]([F:12])[C:2]=4[Cl:1])[N:7]=3)=[CH:16][C:17]1=2)([OH:36])=[O:35]

Participants

3

Reactant 2

HCID 65143-Mercaptopropionic AcidHCID 23359195HCID 23359195, compound

Product 1

HCID 23359128HCID 23359128, compound

Procedure

2-(5-Chloro-6-fluoroquinolin-2-yl)methoxy-11-hydroxy-6,11-dihydrodibenz[b,e]oxepine and 3-mercaptopropionic acid were used and reacted in the same manner as in Example 1 to obtain the title compound.

Workup

  1. customreacted in the same manner as in Example 1

Sources & evidence

ORD record
ord-7e340e6ca3df46a2ab01edc7fff75a8a
Source dataset
uspto-grants-1997_01
Patent number
US05591752

Reaction notes

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