HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-((5,6,7,8-Tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid → HCID 23361336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-((5,6,7,8-Tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid | HCID 15345547 | — |
| Reactant | HCID 23361329 | HCID 23361329 | — |
| Product | HCID 23361336 | HCID 23361336 | — |
Reaction Steps
Employing the same general procedure as for the preparation of 4-[(5,6,7,8-tetrahydro-8,8-dimethyl-5-oxonaphth-2-yl)ethynyl]benzoic acid (Compound 7), 90 mg (0.23 mmol) of ethyl 4-[(7,8-dihydro-8,8-dimethyl-5(6H)-(3-pentylidene)naphth-3-yl)ethynyl]benzoate (Compound 134) was converted to the title compound using 1 ml (1.0 mmol) of LiOH (1M aqueous solution).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591858 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-a65297aaad16461787b69d23099f4eaa |
| Source note | uspto-grants-1997_01 |