HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 18546174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 86754595 | HCID 86754595 | — |
| Product | HCID 18546174 | HCID 18546174 | — |
Reaction Steps
According to the method described for Reference Example 23, methyl (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-butenoate was subjected to reduction with diisobutylaluminum hydride to give (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-buten-1-ol. Recrystallization from ethyl acetate--hexane gave colorless prisms, m.p.126°-127° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-e7802e5ce6604cf19f294767389c8a80 |
| Source note | uspto-grants-1997_01 |