HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (cyanomethyl)phosphonate → HCID 23361383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (cyanomethyl)phosphonate | HCID 75676 | — |
| Reactant | HCID 18546119 | HCID 18546119 | — |
| Product | HCID 23361383 | HCID 23361383 | — |
Reaction Steps
According to the method described for Reference Example 35, (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-buten-1-al was allowed to react with diethyl cyanomethylphosphonate gave (E,E)-5-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2,4-hexadienenitrile. Recrystallization from ethyl acetate--hexane gave colorless prisms, m.p.134°-136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-41e8f0ea0b6c4cc49372dee7454207ec |
| Source note | uspto-grants-1997_01 |