HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propenol → (E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propen-1-al
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propenol | HCID 10860209 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Product | (E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propen-1-al | HCID 11834143 | — |
Reaction Steps
According to the method described for Reference Example 34, (E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propen-1-ol was subjected to oxidation with activated manganese dioxide to give (E)-3-[3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propen-1-al. Recrystallization from ethyl acetate--hexane gave colorless prisms, m.p.103°-104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05591862 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-7bc1c3a8145d4d56b0e0f7d581ecbc0c |
| Source note | uspto-grants-1997_01 |