HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 53857553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | 3,5-Bis(trifluoromethyl)benzaldehyde | HCID 136247 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53857553 | HCID 53857553 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step A of Example 2, using 36.3 grams (0.15 mole) of 3,5-di(trifluoromethyl)benzaldehyde, 22.0 grams (0.17 mole) of ethylacetoacetate, 2 mL of piperidine, and 3 mL of glacial acetic acid in 250 mL of toluene, yielding ethyl 3-oxo-2-[3,5-di(trifluoromethyl)phenylmethylidene]butanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05593998 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-8530f5531aa94286b305af8e603b0d7a |
| Source note | uspto-grants-1997_01 |