HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldiimidazole → HCID 86750190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldiimidazole | HCID 80264 | — |
| Reactant | HCID 69717629 | HCID 69717629 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86750190 | HCID 86750190 | 46% |
Reaction Steps
A solution of 1,1'-thiocarbonyldiimidazole (1.8 g, 20 mmol) and 2-aminonaptho[1,2]thiazole (2.0 g, 20 mmol) in acetonitrile (150 mL) was stirred at 65° C. for 24 h. The resulting precipitate was collected by filtration to provide 1.69 g (46%) of the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05593993 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-6a2fd9e863d54c3381444bbdee7c7a13 |
| Source note | uspto-grants-1997_01 |