Phenethylamine → HCID 86750191, compound

Participants

Reaction Steps

A solution of 1-[(2-naptho[1,2]thiazolyl)thiocarbamoyl]imidazole (1.6 g, 5 mmol) and 2-phenylethylamine (0.62 g, 5.2 mmol) in N,N-dimethylformamide (20 mL) was stirred at 90° C. for 1 h, the reaction was cooled to room temperature and the solvent removed in vacuo. The residue was crystallized from ethyl acetate to provide 1.5 g (82%) of the titled product:

Provenance & Evidence