HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → HCID 23358141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | HCID 12918453 | HCID 12918453 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23358141 | HCID 23358141 | 84.7% |
Reaction Steps
A solution of 2.67 g of 3,4-dichloroaniline in 10 ml of toluene was added to 3.87 g of 2,3-dihydro-5-indenylsulfonylisocyanate in 20 ml of toluene. After stirring 7 hours, the resulting precipitate was recovered by filtration, washed with toluene and dried providing 5.38 g of the title product, m.p. 155.5°-158° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05594028 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-09ac9d0c3c604e9d9f52b09b3734650f |
| Source note | uspto-grants-1997_01 |