HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 10361612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | (+)-Boldine | HCID 10154 | — |
| Product | HCID 10361612 | HCID 10361612 | — |
Reaction Steps
1 g of boldine was dissolved in 30 ml of N,N-dimethylformamide(DMF), the mixture was reacted with 1.2 ml of allyl bromide at 100°-110° C. for 2 hours. The residue obtained after evaporation under reduced pressure was purified to give the pure compound (1) N-allylsecoboldine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05594033 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-d17de981498644e28f737b6cd522b3ba |
| Source note | uspto-grants-1997_01 |