HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1-Decenyl)nitrobenzene → 4-Decylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1-Decenyl)nitrobenzene | HCID 54217323 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-Decylaniline | HCID 92309 | 100.1% |
Reaction Steps
A mixture of 4-(1-decenyl)nitrobenzene (12.2 g), acetic acid (120 ml) and palladium black (0.84 g) was hydrogenated at room temperature and at 3-4 atm for 12 hours. The catalyst was changed and the reaction was continued under the same conditions for 12 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 10.9 g of 4-decylaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05593988 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-1f2c2bdd669143e7b58c28911526e978 |
| Source note | uspto-grants-1997_01 |