HRID234071

反应详情

EQUATION

反应方程式

HRID 234071 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.

WORKUP

后处理

  1. customThe reaction vessel was purged with hydrogen gas
  2. filtrationThe reaction mixture was filtered through Celite
  3. concentrationthe filtrate was concentrated