Sodium Hydroxide → HCID 54409833, compound

HRID 234136Notes

Reaction equation

[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH:11]([CH2:14][CH2:15][C:16]([NH:18][CH2:19][CH2:20][C:21]2[CH:26]=[CH:25][C:24]([O:27][CH2:28][C:29]([O:31]CC)=[O:30])=[C:23]([O:34][CH2:35][C:36]([O:38]CC)=[O:37])[CH:22]=2)=[O:17])[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[OH-].[Na+]>>[C:1]([O:5][C:6]([N:8]1[CH2:9][CH2:10][CH:11]([CH2:14][CH2:15][C:16]([NH:18][CH2:19][CH2:20][C:21]2[CH:26]=[CH:25][C:24]([O:27][CH2:28][C:29]([OH:31])=[O:30])=[C:23]([O:34][CH2:35][C:36]([OH:38])=[O:37])[CH:22]=2)=[O:17])[CH2:12][CH2:13]1)=[O:7])([CH3:4])([CH3:2])[CH3:3]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 53831756HCID 53831756, compound

Product 1

HCID 54409833HCID 54409833, compoundYield 89.6%

Procedure

The compound obtained in the above process (a) (150 mg) was hydrolyzed with 1.3 ml of 1N sodium hydroxide to give 121 mg of the title compound.

Sources & evidence

ORD record: ord-b082e68dc1494bd198c8382f74a93ad6
Source dataset: uspto-grants-1997_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05594004

Reaction notes

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