HRID234384

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID4100861

4-Propylphenylboronic acid

C9H13BO2

HCID23445587

未命名化合物

PRODUCTS

生成物

结构：CCCc1ccc(-c2ccc(S(=O)(=O)n3cccc3)s2)cc1

HCID22998454

未命名化合物

收率 55%

PROCEDURE

实验过程

N-[5-(4-propylphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 33C, from 4-propylphenyl boronic acid and N-(5-bromothiophenesulfonyl)pyrrole. Purification by column chromatography using 10% ethyl acetate/hexanes gave the pure sulfonamide as a white solid in 55% yield, m.p. 106°-108° C.

WORKUP

后处理

customPurification by column chromatography